methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

Base Information

Chemical Name:methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate
CAS No.:935265-51-3
Molecular Formula:C₂₉H₄₀N₂O₄Si
Molecular Weight:508.733
Hs Code.:

Synonyms:methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

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Technology Process of methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

There total 3 articles about methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 935265-51-3
methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

Guidance literature:

Reference yield: 56.0%

: 1-[(tert-butyldimethylsilyl)oxy]-1-(5-tributylstannyloxazol-2-yl)-7-phenylheptane

: 26218-78-0
methyl 6-bromonicotinate

: 935265-51-3
methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 16h; Reflux; Inert atmosphere;
DOI:10.1021/jm401820q

Reference yield:

: 808134-96-5
1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane

: 73781-91-6
6-Chloronicotinic acid methyl ester

: 935265-51-3
methyl 6-(2-(1-((tert-butyldimethylsilyl)oxy)-7-phenylheptyl)oxazol-5-yl)nicotinate

Guidance literature:: 1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane; With tert.-butyl lithium;

With tributyltin chloride;

6-Chloronicotinic acid methyl ester; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 24h; Further stages.; Heating;
DOI:10.1021/jm0611509