1-HYDROXYCYCLOPROPYLMETHYL CARBAMIC ACID T-BUTYL ESTER

Base Information

• Chemical Name: 1-HYDROXYCYCLOPROPYLMETHYL CARBAMIC ACID T-BUTYL ESTER
• CAS No.: 887577-30-2
• Molecular Formula: C9H17 N O3
• Molecular Weight: 187.239
• Mol file: 887577-30-2.mol

Synonyms:TERT-BUTYL (1-HYDROXYCYCLOPROPYL)METHYLCARBAMATE;tert-butyl N-[(1-oxidanylcyclopropyl)methyl]carbamate;1-Hydroxycyclopropylmethyl carbamic acid t-Butyl ester;

Chemical Property of 1-HYDROXYCYCLOPROPYLMETHYL CARBAMIC ACID T-BUTYL ESTER

Chemical Property:

• PSA: 58.56000
• LogP: 1.42690

Purity/Quality:

97% ^*data from raw suppliers

1-[(Boc-amino)methyl]cyclopropanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-HYDROXYCYCLOPROPYLMETHYL CARBAMIC ACID T-BUTYL ESTER

There total 1 articles about 1-HYDROXYCYCLOPROPYLMETHYL CARBAMIC ACID T-BUTYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 1-(aminomethyl)cyclopropan-1-ol (74592-33-9) → tert-butyl N-[(1-hydroxycyclopropyl)methyl]carbamate (887577-30-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; at 20 - 70 ℃;

Reference yield: 82.0%

tert-butyl N-[(1-hydroxycyclopropyl)methyl]carbamate (887577-30-2) + benzyl (2S)-2-(cyanomethyl)-4-[2-methylsulfinyl-7-(1-naphthyl)-6,8-dihydro-5H-pyrido[3,4-d]pyrimidin-4-yl]piperazine-1-carboxylate → C40H45N7O5

Guidance literature:

With sodium t-butanolate; In toluene; at 0 ℃; for 1h; Inert atmosphere;

upstream raw materials:

di-tert-butyl dicarbonate

1-(aminomethyl)cyclopropan-1-ol

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