Technology Process of C22H22F2N4O5
There total 3 articles about C22H22F2N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H24FN5O5;
With
pyridine hydrofluoride; sodium nitrite;
at 0 - 20 ℃;
for 1.16667h;
With
sodium hydrogencarbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 10 °C
1.2: 3 h / 10 °C
2.1: sodium nitrite; pyridine hydrofluoride / 1.17 h / 0 - 20 °C
With
pyridine hydrofluoride; lithium hexamethyldisilazane; sodium nitrite;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2.1: Sandmeyer Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 10 °C
1.2: 3 h / 10 °C
2.1: sodium nitrite; pyridine hydrofluoride / 1.17 h / 0 - 20 °C
With
pyridine hydrofluoride; lithium hexamethyldisilazane; sodium nitrite;
In
tetrahydrofuran; N,N-dimethyl-formamide;
2.1: Sandmeyer Reaction;