9-Deoxo-FK 506

Base Information

Chemical Name:9-Deoxo-FK 506
CAS No.:133951-08-3
Molecular Formula:C₄₄H₇₁NO₁₁
Molecular Weight:790.048
Hs Code.:

Synonyms:9-Deoxo-FK 506

Suppliers and Price of 9-Deoxo-FK 506

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Deoxo-FK 506

Chemical Property:

Purity/Quality:

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Technology Process of 9-Deoxo-FK 506

There total 9 articles about 9-Deoxo-FK 506 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 133941-67-0,144939-86-6,144939-88-8,144939-89-9
24,33-Bis-(t.butyl-dimethylsilyl)-Δ⁹-FK 506

: 133951-08-3
9-Deoxo-FK 506

Guidance literature:: With hydrogen fluoride; In acetonitrile; 0 deg C to r.t.;
DOI:10.1016/S0040-4020(01)90178-4

Reference yield:

: 181229-32-3
9-deoxo-31-O-demethyl-FK₅₀₆

: 133951-08-3
9-Deoxo-FK 506

Guidance literature:: With S-Adenosyl-L-methionine; magnesium sulfate; In aq. phosphate buffer; at 30 ℃; for 3h; pH=7.4;
DOI:10.1021/np4001224

Reference yield:

: 133941-60-3,134002-08-7
24,33-Bis-(t.butyl-dimethylsilyl)-9(R)-dihydro-FK 506-9,10-thiocarbonate

: 133951-08-3
9-Deoxo-FK 506

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / nBu₃SnH, AIBN / toluene / Heating; other substrates

2: 94 percent / 40percent HF / acetonitrile / 0 deg C to r.t.

With 2,2'-azobis(isobutyronitrile); hydrogen fluoride; tri-n-butyl-tin hydride; In toluene; acetonitrile;
DOI:10.1016/S0040-4020(01)90178-4