benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

Base Information

Chemical Name:benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate
CAS No.:138108-61-9
Molecular Formula:C₃₆H₄₃N₅O₈
Molecular Weight:673.766
Hs Code.:

benzyl (S)-3-<<N-<p-<N-(tert-butoxycarbonyl)amidino>benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

Synonyms:benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

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Technology Process of benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

There total 6 articles about benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 138108-61-9
benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Na₂CO₃ / CH₂Cl₂

2: 100 percent / H₂ / Pd/C / ethanol

3: 1.)2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM), 2.) N-methylmorpholine (NMM) / 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00101a017

Reference yield:

: 15535-95-2
4-(aminoiminomethyl)benzoic acid

: 138108-61-9
benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / tetrahydrofuran; dimethylformamide / 20 °C

2: aq. NaHCO₃ / CH₂Cl₂ / 3.5 h

3: aq. Na₂CO₃ / CH₂Cl₂

4: 100 percent / H₂ / Pd/C / ethanol

5: 1.)2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM), 2.) N-methylmorpholine (NMM) / 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h

With 4-methyl-morpholine; thionyl chloride; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; hydrogen; sodium hydrogencarbonate; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00101a017

Reference yield:

: 3-(4-Carbamimidoyl-benzoylamino)-propionic acid benzyl ester

: 138108-61-9
benzyl (S)-3-<benzoyl>-β-alanyl>amino>-3-<(p-methoxyphenethyl)carbamoyl>propionate

Guidance literature:: Multi-step reaction with 3 steps

1: aq. Na₂CO₃ / CH₂Cl₂

2: 100 percent / H₂ / Pd/C / ethanol

3: 1.)2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM), 2.) N-methylmorpholine (NMM) / 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1021/jm00101a017