2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

Base Information

Chemical Name:2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate
CAS No.:1374560-95-8
Molecular Formula:C₂₃H₁₈F₃NO₃S
Molecular Weight:445.462
Hs Code.:

Synonyms:2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

Chemical Property:

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Technology Process of 2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

There total 1 articles about 2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1233199-78-4
(1,1-difluoro-2-isocyanoethyl)(phenyl)sulfane

: 459-57-4
4-fluorobenzaldehyde

: 65-85-0,8013-63-6
benzoic acid

: 1374560-95-8
2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

Guidance literature:: at 20 ℃; Neat (no solvent);
DOI:10.1002/ejoc.201101518

Reference yield: 92.0%

: 1374560-95-8
2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

: 1374561-30-4
2-[2,2-difluoro-2-(phenylsulfonyl)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/ejoc.201101518

Reference yield: 81.0%

: 1374560-95-8
2-[2,2-difluoro-2-(phenylthio)ethylamino]-1-(4-fluorophenyl)-2-oxoethyl benzoate

: 1374561-13-3
2-(2,2-difluoroethylamino)-1-(4-fluorophenyl)-2-oxoethyl benzoate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 7h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201101518