4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Base Information

Chemical Name:4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt
CAS No.:1450916-06-9
Molecular Formula:C₇H₈O₃S*C₁₄H₁₇N₃O₄
Molecular Weight:463.511
Hs Code.:

Synonyms:4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Suppliers and Price of 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

There total 4 articles about 4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1450915-98-6
4-{4-[(R)-5-[(((4-fluorophenyl)methylene)amino)methyl]-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one

: 104-15-4
toluene-4-sulfonic acid

: 1450916-06-9
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Guidance literature:: With water; In ethanol; at 65 ℃;

Reference yield:

: 438056-69-0
4-(4-aminophenyl)morpholin-3-one

: 1450916-06-9
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran; water / 0.5 h / 0 - 50 °C

2.1: lithium tert-butoxide / dichloromethane / 0.17 h / 40 °C

2.2: 18 h / 35 - 45 °C

3.1: water / ethanol / 65 °C

With water; triethylamine; lithium tert-butoxide; In tetrahydrofuran; ethanol; dichloromethane; water;

Reference yield:

: 1313613-18-1
[4-(3-oxo-morpholin-4-yl)phenyl]carbamic acid benzyl ester

: 1450916-06-9
4-{4-[(5R)-5-(aminomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}morpholin-3-one p-toluenesulfonic acid salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium tert-butoxide / dichloromethane / 0.17 h / 40 °C

1.2: 18 h / 35 - 45 °C

2.1: water / ethanol / 65 °C

With water; lithium tert-butoxide; In ethanol; dichloromethane;