n-butyl 2,4,6-trineopentylphenyl sulfoxide

Base Information

• Chemical Name: n-butyl 2,4,6-trineopentylphenyl sulfoxide
• CAS No.: 86563-37-3
• Molecular Formula: C₂₅H₄₄OS
• Molecular Weight: 392.69

Synonyms:n-butyl 2,4,6-trineopentylphenyl sulfoxide

Chemical Property of n-butyl 2,4,6-trineopentylphenyl sulfoxide

Chemical Property:

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Technology Process of n-butyl 2,4,6-trineopentylphenyl sulfoxide

There total 4 articles about n-butyl 2,4,6-trineopentylphenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

n-butyl 2,4,6-trineopentylphenyl sulfide (344567-44-8) → n-butyl 2,4,6-trineopentylphenyl sulfoxide (86563-37-3)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 0.5h;

DOI:10.1021/jo00166a028

Reference yield:

2,4,6-trineopentylbenzenethiol (344867-87-4) → n-butyl 2,4,6-trineopentylphenyl sulfoxide (86563-37-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, room temp., 30 min, 2.) room temp., 8 h

2: 60 percent / 85percent m-chloroperbenzoic acid / CHCl₃ / 0.5 h

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In chloroform;

DOI:10.1021/jo00166a028

Reference yield:

C21H35BrMg → n-butyl 2,4,6-trineopentylphenyl sulfoxide (86563-37-3)

Guidance literature:

Multi-step reaction with 4 steps

1: 1.) sulfur, 2.) Et₃N, I₂ / 1.) THF, 12 h, reflux, 2.) CH₃OH

2: LiAlH₄ / tetrahydrofuran / 1 h / Heating

3: 1.) NaH / 1.) THF, room temp., 30 min, 2.) room temp., 8 h

4: 60 percent / 85percent m-chloroperbenzoic acid / CHCl₃ / 0.5 h

With lithium aluminium tetrahydride; iodine; sodium hydride; sulfur; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform;

DOI:10.1021/jo00166a028

upstream raw materials:

n-butyl 2,4,6-trineopentylphenyl sulfide

2,4,6-trineopentylbenzenethiol

bis(2,4,6-trineopentylphenyl) disulfide

Downstream raw materials:

2,4,6-trineopentylbenzenethiol

2-tert-butyl-4,6-dineopentylbenzothiete

3,3-dimethyl-4,4-dihydro-6,8-dineopentylbenzothiapyran

bis(2,4,6-trineopentylphenyl) disulfide

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