2-hydroxy-1,3-xylyl-24-crown-7

Base Information

Chemical Name:2-hydroxy-1,3-xylyl-24-crown-7
CAS No.:116748-80-2
Molecular Formula:C₂₀H₃₂O₈
Molecular Weight:400.469
Hs Code.:

Synonyms:2-hydroxy-1,3-xylyl-24-crown-7

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Chemical Property of 2-hydroxy-1,3-xylyl-24-crown-7

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Technology Process of 2-hydroxy-1,3-xylyl-24-crown-7

There total 1 articles about 2-hydroxy-1,3-xylyl-24-crown-7 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1167462-12-5
C₁₆H₁₅N₃O₅*C₂₀H₃₂O₈

: C₁₆H₁₅N₃O₅

: 116748-80-2
2-hydroxy-1,3-xylyl-24-crown-7

Guidance literature:: In dimethylsulfoxide-d6; at 99.84 - 129.84 ℃; Kinetics; Thermodynamic data;
DOI:10.1016/j.tetlet.2009.02.179

Reference yield: 37.0%

: 116748-80-2
2-hydroxy-1,3-xylyl-24-crown-7

: 99-33-2
3,5-dinitrobenoyl chloride

: 1167462-02-3
C₂₇H₃₄N₂O₁₃

Guidance literature:: 2-hydroxy-1,3-xylyl-24-crown-7; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

3,5-dinitrobenoyl chloride; In tetrahydrofuran; at 20 ℃; for 96h; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.02.179

Reference yield:

: 116748-80-2
2-hydroxy-1,3-xylyl-24-crown-7

: 946533-40-0
C₂₇H₃₃N₃O₁₅

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / sodium nitrite; aq. nitric acid / CHCl₃ / 17 h / 20 °C

2: 64 percent / t-BuOK / tetrahydrofuran / 1 h / 20 °C

With potassium tert-butylate; nitric acid; sodium nitrite; In tetrahydrofuran; chloroform;
DOI:10.1021/ol070999w