N,N-di-2-propenyl benzenecarbothioamide

Base Information

• Chemical Name: N,N-di-2-propenyl benzenecarbothioamide
• CAS No.: 705261-75-2
• Molecular Formula: C₁₃H₁₅NS
• Molecular Weight: 217.335
• Mol file: 705261-75-2.mol

Synonyms:N,N-di-2-propenyl benzenecarbothioamide

Chemical Property of N,N-di-2-propenyl benzenecarbothioamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N,N-di-2-propenyl benzenecarbothioamide

There total 1 articles about N,N-di-2-propenyl benzenecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N,N-diallylbenzamide (10283-70-2) → N,N-di-2-propenyl benzenecarbothioamide (705261-75-2)

Guidance literature:

N,N-diallylbenzamide; With oxalyl dichloride; In diethyl ether; at 0 - 20 ℃;

With lithium aluminium tetrahydride; sulfur; In tetrahydrofuran; diethyl ether; at 20 ℃; for 3h;

DOI:10.1021/ja048627v

Reference yield: 71.0%

1-(2-(Penta-1,3-diyn-1-yl)phenyl)-3-(trimethylsilyl)prop-2-yn-1-one (1461737-53-0) + N,N-di-2-propenyl benzenecarbothioamide (705261-75-2) → 2-allyl-5-methyl-1-phenyl-6-(trimethylsilyl)-3-vinyl-2,3-dihydrofluoreno[4,3-e][1,3]thiazin-7(1H)-one

Guidance literature:

In benzene; at 90 ℃; for 12h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.6b03199

Reference yield: 66.0%

N-(hepta-3,5-diyn-1-yl)-4-methyl-N-(penta-1,3-diyn-1-yl)benzenesulfonamide + N,N-di-2-propenyl benzenecarbothioamide (705261-75-2) → 8-allyl-5-methyl-9-phenyl-4-(prop-1-yn-1-yl)-1-tosyl-7-vinyl-1,2,3,7,8,9-hexahydro-[1,3]thiazino[6,5-g]indole

Guidance literature:

In benzene; at 90 ℃; for 12h; regioselective reaction; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.6b03199

upstream raw materials:

N,N-diallylbenzamide