(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

Base Information

Chemical Name:(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene
CAS No.:135145-83-4
Molecular Formula:C₃₉H₇₄O₄Si₃
Molecular Weight:691.271
Hs Code.:

Synonyms:(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

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Chemical Property of (1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

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Technology Process of (1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

There total 12 articles about (1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-86-1,52753-63-6
bromobenzene

: 1200443-31-7
(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)boronic acid pinacol ester

: 135145-83-4
(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; water; for 3h; Reflux;
DOI:10.1016/j.tet.2012.05.035

Reference yield: 90.0%

: 28557-00-8
phenylzinc chloride

: 135145-81-2
3,4,6-tri-O-triisopropylsilyl-1-iodo-D-glucal

: 135145-83-4
(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

Guidance literature:: bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1021/jo00016a003

Reference yield: 89.0%

: 108-86-1,52753-63-6
bromobenzene

: 1355014-76-4
(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)boronic acid

: 135145-83-4
(1,5-anhydro-2-deoxy-3,4,6-tris-O-triisopropylsilyl-D-arabino-hex-1-enitolyl)benzene

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In 1,2-dimethoxyethane; water; at 60 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201304304