Technology Process of C19H14Br2N2S2
There total 3 articles about C19H14Br2N2S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H16N2S2;
With
acetic acid;
In
benzene;
Inert atmosphere;
With
N-Bromosuccinimide;
In
benzene;
for 4h;
Inert atmosphere;
Reflux;
With
sodium hydroxide;
In
water; benzene;
Inert atmosphere;
DOI:10.1016/j.dyepig.2011.08.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: ammonium acetate; acetic acid / 1 h / Inert atmosphere; Reflux
1.2: Inert atmosphere; Reflux
1.3: Cooling; Inert atmosphere
2.1: acetic acid / benzene / Inert atmosphere
2.2: 4 h / Inert atmosphere; Reflux
2.3: Inert atmosphere
With
ammonium acetate; acetic acid;
In
benzene;
DOI:10.1016/j.dyepig.2011.08.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / carbon disulfide / Inert atmosphere
2.1: ammonium acetate; acetic acid / 1 h / Inert atmosphere; Reflux
2.2: Inert atmosphere; Reflux
2.3: Cooling; Inert atmosphere
3.1: acetic acid / benzene / Inert atmosphere
3.2: 4 h / Inert atmosphere; Reflux
3.3: Inert atmosphere
With
aluminum (III) chloride; ammonium acetate; acetic acid;
In
carbon disulfide; benzene;
DOI:10.1016/j.dyepig.2011.08.005