1-(5-Bromo-2-methoxyphenyl)ethanol

Base Information

Chemical Name:1-(5-Bromo-2-methoxyphenyl)ethanol
CAS No.:16602-17-8
Molecular Formula:C9H11 Br O2
Molecular Weight:231.089
Hs Code.:2909499000
DSSTox Substance ID:DTXSID60501902
Mol file:16602-17-8.mol

Synonyms:1-(5-BROMO-2-METHOXYPHENYL)ETHANOL;16602-17-8;1-(5-bromo-2-methoxyphenyl)ethan-1-ol;BENZENEMETHANOL, 5-BROMO-2-METHOXY-A-METHYL-;5-Bromo-2-methoxy-alpha-methyl-benzenemethanol;SCHEMBL7426724;DTXSID60501902;WNRYFLFXINLLKQ-UHFFFAOYSA-N;AKOS005135655;1-(5-bromo-2-methoxy-phenyl)-ethanol;W19098;A810688;F2185-0062

Suppliers and Price of 1-(5-Bromo-2-methoxyphenyl)ethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(5-Bromo-2-methoxyphenyl)ethanol 95+%
5g
$ 746.00

Chemenu
1-(5-Bromo-2-methoxyphenyl)ethanol 95%
5g
$ 704.00

Alichem
1-(5-Bromo-2-methoxyphenyl)ethanol
1g
$ 209.09

Total 5 raw suppliers

Chemical Property of 1-(5-Bromo-2-methoxyphenyl)ethanol

Chemical Property:

Boiling Point:320.1±32.0 °C(Predicted)
PKA:14.20±0.20(Predicted)
PSA：29.46000
Density:1.438±0.06 g/cm3(Predicted)
LogP:2.51100
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:229.99424
Heavy Atom Count:12
Complexity:141

Purity/Quality:

97% ^*data from raw suppliers

1-(5-Bromo-2-methoxyphenyl)ethanol 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C1=C(C=CC(=C1)Br)OC)O

Technology Process of 1-(5-Bromo-2-methoxyphenyl)ethanol

There total 5 articles about 1-(5-Bromo-2-methoxyphenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 16740-73-1
5-bromo-2-methoxyacetophenone

: 16602-17-8
1-(5-bromo-2-methoxyphenyl)-1-ethanol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 1h;
DOI:10.1016/j.ejmech.2017.12.071

Reference yield:

: 1761-61-1
5-bromosalicyclaldehyde

: 16602-17-8
1-(5-bromo-2-methoxyphenyl)-1-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide

2: tetrahydrofuran

With potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1124/dmd.112.046870

Reference yield:

: 1450-75-5
5-Bromo-2-hydroxyacetophenone

: 16602-17-8
1-(5-bromo-2-methoxyphenyl)-1-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: sodium tetrahydroborate / methanol / 1 h / 0 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2017.12.071