p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

Base Information

Chemical Name:p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside
CAS No.:870543-44-5
Molecular Formula:C₁₉H₂₄O₉
Molecular Weight:396.394
Hs Code.:

Synonyms:p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

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Technology Process of p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

There total 3 articles about p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 3615-37-0,478518-52-4
D-Fucose

: 108-24-7
acetic anhydride

: 150-76-5
4-methoxy-phenol

: 870543-44-5
p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

Guidance literature:: D-Fucose; acetic anhydride; With pyridine; for 12h;

4-methoxy-phenol; With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1002/anie.200502615

Reference yield:

: 51921-33-6
1,2,3,4-tetra-O-acetyl-D-fucopyranose

: 150-76-5
4-methoxy-phenol

: 870543-44-5
p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201712022

Reference yield:

: 73-34-7,87-96-7,488-79-9,551-63-3,609-01-8,643-17-4,643-18-5,4164-09-4,6014-42-2,6155-36-8,6189-71-5,6696-41-9,6736-43-2,13224-93-6,22611-09-2,28161-49-1,28161-50-4,28161-52-6,45864-36-6,63814-64-2,71116-59-1,71116-61-5,72598-05-1,87936-88-7,87936-89-8,97466-79-0,116908-82-8,120442-60-6,123484-22-0,133576-32-6
D-Fucose

: 870543-44-5
p-methoxy phenyl-2,3,4-tri-O-acetyl-α-D-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 10 h / 0 - 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1002/anie.201712022