(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

Base Information

Chemical Name:(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester
CAS No.:134005-45-1
Molecular Formula:C₁₇H₂₄Cl₂O₃
Molecular Weight:347.282
Hs Code.:

Synonyms:(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

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Chemical Property of (S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

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Technology Process of (S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

There total 6 articles about (S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134005-34-8
(R)-ε-<2-(benzyloxy)ethyl>-ε-caprolactone

: 134005-45-1
(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / LiAlH₄ / diethyl ether / 1.) RT, 30 min, 2.) reflux, 3 h

2: H₂ / 10percent Pd/C / aq. ethanol / 48 h / 2792.6 Torr / Ambient temperature

3: 59 percent / triphenylphosphine, CCl₄ / 18 h / Heating

4: DCC, DMAP / tetrahydrofuran / 18 h / Ambient temperature

With tetrachloromethane; dmap; lithium aluminium tetrahydride; hydrogen; dicyclohexyl-carbodiimide; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1021/jm00111a026

Reference yield:

: 134005-35-9
(R)-1-O-benzyl-1,3,8-octanetriol

: 134005-45-1
(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / aq. ethanol / 48 h / 2792.6 Torr / Ambient temperature

2: 59 percent / triphenylphosphine, CCl₄ / 18 h / Heating

3: DCC, DMAP / tetrahydrofuran / 18 h / Ambient temperature

With tetrachloromethane; dmap; hydrogen; dicyclohexyl-carbodiimide; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00111a026

Reference yield:

: 134005-37-1
(R)-1,8-di-O-benzyl-1,3,8-octanetriol

: 134005-45-1
(S)-Methoxy-phenyl-acetic acid (R)-6-chloro-1-(2-chloro-ethyl)-hexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 50 h / 2585.7 Torr / Ambient temperature

2: 59 percent / triphenylphosphine, CCl₄ / 18 h / Heating

3: DCC, DMAP / tetrahydrofuran / 18 h / Ambient temperature

With tetrachloromethane; dmap; hydrogen; dicyclohexyl-carbodiimide; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00111a026