(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

Base Information

Chemical Name:(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene
CAS No.:1044749-80-5
Molecular Formula:C₂₄H₄₂O₅Si
Molecular Weight:438.68
Hs Code.:

Synonyms:(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

Suppliers and Price of (E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of (E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of (E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

There total 1 articles about (E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1044749-61-2
(Z)-1-bromo-2-(triisopropylsilyloxymethyl)but-2-ene

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 1044749-80-5
(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1016/j.tetasy.2008.04.025

Reference yield: 79.0%

: 1044749-80-5
(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

: (1RS,2SR)-2-methyl-3-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxyphenyl)but-3-en-1-ol

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/j.tetasy.2008.04.025

Reference yield:

: 1044749-80-5
(E)-2-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxybenzyloxy)but-2-ene

: 1044750-03-9
(1R,2S)-2-methyl-3-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxyphenyl)but-3-en-1-ol

: (1S,2R)-2-methyl-3-(triisopropylsilyloxymethyl)-1-(3,4,5-trimethoxyphenyl)but-3-en-1-ol

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 2h; Title compound not separated from byproducts.;
DOI:10.1016/j.tetasy.2008.04.025