C₂₅H₃₂O₇

Base Information

Chemical Name:C₂₅H₃₂O₇
CAS No.:1362110-35-7
Molecular Formula:C₂₅H₃₂O₇
Molecular Weight:444.525
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₂O₇

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Chemical Property of C₂₅H₃₂O₇

Chemical Property:

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Technology Process of C₂₅H₃₂O₇

There total 12 articles about C₂₅H₃₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1362110-33-5
C₂₅H₃₀O₆

: 1362110-35-7
C₂₅H₃₂O₇

Guidance literature:: C₂₅H₃₀O₆; With ammonia; In methanol; water; at 66 ℃; for 6h;

With hydrogenchloride; In methanol; water; ethyl acetate; at 0 ℃; pH=2;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-25-5
C₃₂H₄₇IO₄Si

: 1362110-35-7
C₂₅H₃₂O₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: tert.-butyl lithium / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

1.2: brine

2.1: Burgess Reagent / tetrahydrofuran / 20 - 50 °C / Inert atmosphere

3.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

4.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

5.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

7.2: brine

8.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

9.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

10.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

11.1: ammonia / methanol; water / 6 h / 66 °C

11.2: 0 °C / pH 2

With 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; Burgess Reagent; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Barbier type cyclization / 8.1: Sharpless epoxidation;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-27-7
C₃₂H₄₆O₃Si

: 1362110-35-7
C₂₅H₃₂O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

3.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: brine

6.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

9.1: ammonia / methanol; water / 6 h / 66 °C

9.2: 0 °C / pH 2

With 1H-imidazole; tert.-butylhydroperoxide; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; N,N-dimethyl-formamide; 6.1: Sharpless epoxidation;
DOI:10.1021/ol300390k