4-hydroxy-2,3-dimethylphenyl allyl ether

Base Information

• Chemical Name: 4-hydroxy-2,3-dimethylphenyl allyl ether
• CAS No.: 3732-03-4
• Molecular Formula: C₁₁H₁₄O₂
• Molecular Weight: 178.231
• Mol file: 3732-03-4.mol

Synonyms:4-hydroxy-2,3-dimethylphenyl allyl ether

Chemical Property of 4-hydroxy-2,3-dimethylphenyl allyl ether

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-hydroxy-2,3-dimethylphenyl allyl ether

There total 2 articles about 4-hydroxy-2,3-dimethylphenyl allyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

allyl bromide (106-95-6) + 2,3-dimethyl-1,4-dihydroxybenzene (608-43-5) → 4-hydroxy-2,3-dimethylphenyl allyl ether (3732-03-4) + 1,4-bis(allyloxy)-2,3-dimethylbenzene (332426-35-4)

Guidance literature:

With potassium carbonate; In acetone; for 18h; Heating;

DOI:10.1021/jo0301090

Reference yield: 35.0%

allyl bromide (106-95-6) + 2,3-dimethyl-1,4-dihydroxybenzene (608-43-5) → 4-hydroxy-2,3-dimethylphenyl allyl ether (3732-03-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;

DOI:10.1021/jm9603633

Reference yield: 81.0%

4-hydroxy-2,3-dimethylphenyl allyl ether (3732-03-4) → 6-allyl-2,3-dimethylbenzene-1,4-diol (66557-15-1)

Guidance literature:

In decalin; at 190 - 195 ℃; for 5h;

DOI:10.1021/jo0301090

upstream raw materials:

allyl bromide

2,3-dimethyl-1,4-dihydroxybenzene

Downstream raw materials:

6-allyl-2,3-dimethylbenzene-1,4-diol

(4-Allyloxy-2,3-dimethyl-phenoxy)-tert-butyl-dimethyl-silane

5-hydroxy-2,6,7-trimethyl-2,3-dihydrobenzofuran-4-carbaldehyde

6-Allyl-4-(tert-butyl-dimethyl-silanyloxy)-2,3-dimethyl-phenol