1-(3-Iodo-4-methylphenyl)ethanone

Base Information

Chemical Name:1-(3-Iodo-4-methylphenyl)ethanone
CAS No.:52107-84-3
Molecular Formula:C9H9IO
Molecular Weight:260.074
Hs Code.:2914700090
DSSTox Substance ID:DTXSID70553699
Nikkaji Number:J3.656.182C
Wikidata:Q82434355
Mol file:52107-84-3.mol

Synonyms:1-(3-IODO-4-METHYLPHENYL)ETHANONE;52107-84-3;1-(3-Iodo-4-methylphenyl)ethan-1-one;Ethanone,1-(3-iodo-4-methylphenyl)-;SCHEMBL17325043;DTXSID70553699;CCA10784;A828925

Suppliers and Price of 1-(3-Iodo-4-methylphenyl)ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(3-Iodo-4-methylphenyl)ethanone 95+%
5g
$ 746.00

American Custom Chemicals Corporation
1-(3-IODO-4-METHYLPHENYL)ETHANONE 95.00%
5MG
$ 500.07

Alichem
1-(3-Iodo-4-methylphenyl)ethanone
1g
$ 217.21

Total 8 raw suppliers

Chemical Property of 1-(3-Iodo-4-methylphenyl)ethanone

Chemical Property:

Boiling Point:306.516 °C at 760 mmHg
Flash Point:139.176 °C
PSA：17.07000
Density:1.632 g/cm³
LogP:2.80220
Storage Temp.:2-8°C
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:259.96981
Heavy Atom Count:11
Complexity:156

Purity/Quality:

98%, ^*data from raw suppliers

1-(3-Iodo-4-methylphenyl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1)C(=O)C)I

Technology Process of 1-(3-Iodo-4-methylphenyl)ethanone

There total 5 articles about 1-(3-Iodo-4-methylphenyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 122-00-9
para-methylacetophenone

: 52107-84-3
1-(3-iodo-4-methylphenyl)ethan-1-one

Guidance literature:: With iodine tris(trifluoroacetate); In dichloromethane; for 7h; Ambient temperature;
DOI:10.1246/bcsj.60.4363

Reference yield: 67.0%

: 2089-33-0
4-methylacethophenone oxime

: 52107-84-3
1-(3-iodo-4-methylphenyl)ethan-1-one

: 122-00-9
para-methylacetophenone

Guidance literature:: With iodic acid; In dichloromethane; at 20 ℃; for 11h;
DOI:10.1016/S0040-4039(02)00710-4

Reference yield:

: 42872-79-7
3-iodo-4-methylbenzonitrile

: 52107-84-3
1-(3-iodo-4-methylphenyl)ethan-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: aq. NaOH

2: SOCl₂

3: (i), (ii) (hydrolysis), (iii) (decarboxylation)

With sodium hydroxide; thionyl chloride;