dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide

Base Information

• Chemical Name: dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide
• CAS No.: 610778-62-6
• Molecular Formula: C₁₈H₁₉IN₂S*HI
• Molecular Weight: 550.245
• Mol file: 610778-62-6.mol

Synonyms:dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide

Chemical Property of dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide

There total 2 articles about dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H20N2S → dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide (610778-62-6)

Guidance literature:

With iodine; In methanol; at 20 ℃; for 24h;

DOI:10.1016/j.bmc.2016.01.031

Reference yield:

dibenzylamine (103-49-1) → dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide (610778-62-6)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 20 °C

2: iodine / methanol / 24 h / 20 °C

With iodine; In methanol; diethyl ether;

DOI:10.1016/j.bmc.2016.01.031

Reference yield: 96.0%

dibenzyl-(5-iodomethyl-4,5-dihydro-thiazol-2-yl)amine hydroiodide (610778-62-6) → 2-(N,N-dibenzyl)amino-5-hydroxymethylthiazoline (899589-91-4)

Guidance literature:

With water; lead(II) oxide; In ethanol; at 80 ℃; for 4h;

DOI:10.1007/s10593-007-0054-5

upstream raw materials:

dibenzylamine

Downstream raw materials:

2-(N,N-dibenzyl)amino-5-hydroxymethylthiazoline