C₅₈H₆₀N₄O₂₀S₂

Base Information

Chemical Name:C₅₈H₆₀N₄O₂₀S₂
CAS No.:1262795-82-3
Molecular Formula:C₅₈H₆₀N₄O₂₀S₂
Molecular Weight:1197.26
Hs Code.:

C<sub>58</sub>H<sub>60</sub>N<sub>4</sub>O<sub>20</sub>S<sub>2</sub>

Synonyms:C₅₈H₆₀N₄O₂₀S₂

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Chemical Property of C₅₈H₆₀N₄O₂₀S₂

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Technology Process of C₅₈H₆₀N₄O₂₀S₂

There total 11 articles about C₅₈H₆₀N₄O₂₀S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1262795-75-4
C₂₉H₃₀N₂O₁₀S

: 1262795-82-3
C₅₈H₆₀N₄O₂₀S₂

Guidance literature:: With palladium(II) acetate; triphenylphosphine; In benzene; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1071/CH10359

Reference yield:

: 1262795-73-2
C₂₆H₂₈N₂O₁₀S

: 1262795-82-3
C₅₈H₆₀N₄O₂₀S₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 18 °C / Inert atmosphere

2.1: palladium(II) acetate; triphenylphosphine / benzene / 2 h / 80 °C / Inert atmosphere

With palladium(II) acetate; sodium hydride; triphenylphosphine; In N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1071/CH10359

Reference yield:

: 1027032-85-4
C₁₂H₂₀O₂

: 1262795-82-3
C₅₈H₆₀N₄O₂₀S₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 3 h / 40 °C / Inert atmosphere

2.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / dichloromethane; water / 4 h / 18 °C / Inert atmosphere

3.1: 1,4-dioxane / 18 h / 80 °C

4.1: 1,4-dioxane / 24 h / 105 °C

5.1: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 3 h / 0 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 2 h / 18 °C / Inert atmosphere

7.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; caesium carbonate / tetrahydrofuran; water / 2 h / 65 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.5 h / 0 °C / Inert atmosphere

8.2: 2 h / 0 - 18 °C / Inert atmosphere

9.1: palladium(II) acetate; triphenylphosphine / benzene / 2 h / 80 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; trimethylsilyl trifluoromethanesulfonate; palladium(II) acetate; N-benzyl-N,N,N-triethylammonium chloride; potassium acetate; sodium hydride; caesium carbonate; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene; 7.1: Suzuki coupling;
DOI:10.1071/CH10359