C₄₁H₆₁NO₁₁SSi₂

Base Information

Chemical Name:C₄₁H₆₁NO₁₁SSi₂
CAS No.:1622094-30-7
Molecular Formula:C₄₁H₆₁NO₁₁SSi₂
Molecular Weight:832.172
Hs Code.:

C<sub>41</sub>H<sub>61</sub>NO<sub>11</sub>SSi<sub>2</sub>

Synonyms:C₄₁H₆₁NO₁₁SSi₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₆₁NO₁₁SSi₂

Chemical Property:

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Technology Process of C₄₁H₆₁NO₁₁SSi₂

There total 16 articles about C₄₁H₆₁NO₁₁SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1622094-38-5
C₄₁H₆₁NO₉SSi₂

: 1622094-30-7
C₄₁H₆₁NO₁₁SSi₂

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201402323

Reference yield:

: 1622094-37-4
C₄₀H₆₁NO₈SSi₂

: 1622094-30-7
C₄₁H₆₁NO₁₁SSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: lithium iodide monohydrate / ethyl acetate / 8 h / 20 °C / Reflux

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

With dmap; lithium iodide monohydrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ethyl acetate;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-30-7
C₄₁H₆₁NO₁₁SSi₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2.1: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

3.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

4.1: water; tetrahydrofuran / 0.08 h

4.2: 2 h / 0 °C

5.1: lithium iodide monohydrate / ethyl acetate / 48 h / 20 °C / Reflux

6.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0.17 h / 20 °C

7.1: potassium hydroxide / water; methanol / 0.25 h / -20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

11.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

12.1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

13.1: lithium iodide monohydrate / ethyl acetate / 8 h / 20 °C / Reflux

14.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetonitrile; 4.1: |Schotten-Baumann Reaction;
DOI:10.1002/chem.201402323