1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

Base Information

Chemical Name:1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene
CAS No.:934824-84-7
Molecular Formula:C₅₄H₅₄N₆O₉
Molecular Weight:931.058
Hs Code.:

Synonyms:1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

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Chemical Property of 1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

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Technology Process of 1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

There total 1 articles about 1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848352-99-8
5-(benzyloxycarbonyl)-1H-pyrrole-2-carboxylic acid

: 1,3,5-tris(aminomethyl)-2,4,6-triethylbenzene trihydrochloride

: 934824-84-7
1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

Guidance literature:: With dmap; sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 4-methyl-morpholine; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1021/ja0433469

Reference yield:

: 934824-84-7
1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

: 848353-00-4
1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid)-2,4,6-triethylbenzene

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; at 40 ℃; for 3h;
DOI:10.1021/ja0433469

Reference yield:

: 934824-84-7
1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carboxylic acid benzyl ester)-2,4,6-triethylbenzene

: 1,3,5-tris(5-ethylcarbamoyl-1H-pyrrole-2-carbonylguanidine)-2,4,6-triethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 0.05 g / H₂ / Pd/C / methanol; tetrahydrofuran / 3 h / 40 °C

2: N-methylmorpholine; PyBOP / dimethylformamide

3: TFA / CH₂Cl₂ / 20 °C

With 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0433469