2-methyl-2-(benzylthiomethyl)malonic diacid

Base Information

Chemical Name:2-methyl-2-(benzylthiomethyl)malonic diacid
CAS No.:366490-38-2
Molecular Formula:C₁₂H₁₄O₄S
Molecular Weight:254.307
Hs Code.:

Synonyms:2-methyl-2-(benzylthiomethyl)malonic diacid

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Chemical Property of 2-methyl-2-(benzylthiomethyl)malonic diacid

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Technology Process of 2-methyl-2-(benzylthiomethyl)malonic diacid

There total 3 articles about 2-methyl-2-(benzylthiomethyl)malonic diacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 256505-79-0
diethyl 2-(benzylthiomethyl)-2-methylmalonate

: 366490-38-2
2-methyl-2-(benzylthiomethyl)malonic diacid

Guidance literature:: With potassium hydroxide; In ethanol; water; at 25 ℃; for 72h;
DOI:10.1081/SCC-100104041

Reference yield:

: 3970-13-6
benzyl chloromethyl sulfide

: 366490-38-2
2-methyl-2-(benzylthiomethyl)malonic diacid

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / NaH / dimethylformamide / -10 - 25 °C

2: 99 percent / potassium hydroxide / ethanol; H₂O / 72 h / 25 °C

With potassium hydroxide; sodium hydride; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104041

Reference yield:

: 100-53-8
phenylmethanethiol

: 366490-38-2
2-methyl-2-(benzylthiomethyl)malonic diacid

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / potassium hydroxide; triethylbenzylammonium chloride / 1 h / 20 °C

2: 75 percent / NaH / dimethylformamide / -10 - 25 °C

3: 99 percent / potassium hydroxide / ethanol; H₂O / 72 h / 25 °C

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; sodium hydride; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1081/SCC-100104041