C₃₂H₅₃SiNO₈

Base Information

Chemical Name:C₃₂H₅₃SiNO₈
CAS No.:937163-90-1
Molecular Formula:C₃₂H₅₃NO₈Si
Molecular Weight:607.86
Hs Code.:

C<sub>32</sub>H<sub>53</sub>SiNO<sub>8</sub>

Synonyms:C₃₂H₅₃SiNO₈

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Chemical Property of C₃₂H₅₃SiNO₈

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Technology Process of C₃₂H₅₃SiNO₈

There total 13 articles about C₃₂H₅₃SiNO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 937163-88-7
C₃₂H₅₃SiNO₈

: 937163-90-1
C₃₂H₅₃SiNO₈

Guidance literature:: With triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; at 40 ℃; for 12h;
DOI:10.1021/ol070435s

Reference yield:

: 937164-11-9
C₂₄H₃₈SiO₅

: 937163-90-1
C₃₂H₅₃SiNO₈

Guidance literature:: Multi-step reaction with 10 steps

1: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

2: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

3: 82 percent / NIS / CH₂Cl₂ / 20 °C

4: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

5: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

6: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

7: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

8: 95 percent / K₂CO₃ / methanol / 20 °C

9: 89 percent / CeCl₃*7H₂O; NaBH₄ / CH₂Cl₂; methanol / 1 h / -78 °C

10: 83 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 12 h / 40 °C

With sodium tetrahydroborate; N-iodo-succinimide; cerium(III) chloride; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; diisobutylaluminium hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile; 9: Luche reduction;
DOI:10.1021/ol070435s

Reference yield:

: 937163-73-0
C₁₇H₃₄SiO₄

: 937163-90-1
C₃₂H₅₃SiNO₈

Guidance literature:: Multi-step reaction with 9 steps

1: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

2: 82 percent / NIS / CH₂Cl₂ / 20 °C

3: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

4: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

5: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

6: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

7: 95 percent / K₂CO₃ / methanol / 20 °C

8: 89 percent / CeCl₃*7H₂O; NaBH₄ / CH₂Cl₂; methanol / 1 h / -78 °C

9: 83 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 12 h / 40 °C

With sodium tetrahydroborate; N-iodo-succinimide; cerium(III) chloride; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile; 8: Luche reduction;
DOI:10.1021/ol070435s