C₃₆H₅₂N₂O₅

Base Information

Chemical Name:C₃₆H₅₂N₂O₅
CAS No.:205386-10-3
Molecular Formula:C₃₆H₅₂N₂O₅
Molecular Weight:592.819
Hs Code.:

C<sub>36</sub>H<sub>52</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₆H₅₂N₂O₅

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Chemical Property of C₃₆H₅₂N₂O₅

Chemical Property:

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Technology Process of C₃₆H₅₂N₂O₅

There total 19 articles about C₃₆H₅₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 205386-08-9
C₂₄H₃₈N₂O₃

: 155137-33-0
benzyl D-2-trifluoromethylsulphonyloxy-3-methylbutanoate

: 205386-10-3
C₃₆H₅₂N₂O₅

Guidance literature:: With 2,6-dimethylpyridine; In 1,2-dichloro-ethane; for 48h; Heating;
DOI:10.1021/jm970704s

Reference yield:

: 637-59-2
1-Bromo-3-phenylpropane

: 205386-10-3
C₃₆H₅₂N₂O₅

Guidance literature:: Multi-step reaction with 18 steps

1: 1.) Mg / 1.) ether, reflux, 2.) ether, RT, 1h

2: 68 percent / 85percent aq. H₂SO₄ / 0.5 h / Ambient temperature

3: CrO₃, aq. AcOH / 1.5 h

4: AlCl₃, Br₂ / CH₂Cl₂ / 1 h

5: 100 percent / CF₃COOH, triethylsilane / 19 h / 0 - 20 °C

6: 1.) n-BuLi / 1.) ether, hexane, RT, 40 min, 2.) ether, hexane, 0 def C, 20 min

7: NaBH₄ / methanol / 0.5 h / 0 °C

8: CHBr₃, Ph₃P / CH₂Cl₂ / 0.25 h / 0 °C

9: 40 percent / fuming HNO₃, AcOH, Ac₂O / 0.33 h / 0 °C

10: 94 percent / NaH / dimethylformamide / 2.5 h / Ambient temperature

11: conc. aq. HCl / acetic acid / 14 h / Heating

12: SOCl₂ / 20 h / Ambient temperature

13: CH₂Cl₂ / 18 h / Ambient temperature

14: LiBH₄ / tetrahydrofuran / 19 h / 0 - 20 °C

15: H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr / Ambient temperature

16: acetic anhydride / tetrahydrofuran / 2 h / 60 - 70 °C

17: BH₃ / tetrahydrofuran / 3 h / 0 °C

18: 83 percent / 2,6-lutidine / 1,2-dichloro-ethane / 48 h / Heating

With 2,6-dimethylpyridine; chromium(VI) oxide; hydrogenchloride; triethylsilane; sodium tetrahydroborate; lithium borohydride; n-butyllithium; aluminium trichloride; thionyl chloride; Bromoform; sulfuric acid; borane; hydrogen; bromine; nitric acid; acetic anhydride; sodium hydride; magnesium; acetic acid; triphenylphosphine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm970704s

Reference yield:

: 101100-11-2
1-(3-phenylpropyl)cyclohexanol

: 205386-10-3
C₃₆H₅₂N₂O₅

Guidance literature:: Multi-step reaction with 17 steps

1: 68 percent / 85percent aq. H₂SO₄ / 0.5 h / Ambient temperature

2: CrO₃, aq. AcOH / 1.5 h

3: AlCl₃, Br₂ / CH₂Cl₂ / 1 h

4: 100 percent / CF₃COOH, triethylsilane / 19 h / 0 - 20 °C

5: 1.) n-BuLi / 1.) ether, hexane, RT, 40 min, 2.) ether, hexane, 0 def C, 20 min

6: NaBH₄ / methanol / 0.5 h / 0 °C

7: CHBr₃, Ph₃P / CH₂Cl₂ / 0.25 h / 0 °C

8: 40 percent / fuming HNO₃, AcOH, Ac₂O / 0.33 h / 0 °C

9: 94 percent / NaH / dimethylformamide / 2.5 h / Ambient temperature

10: conc. aq. HCl / acetic acid / 14 h / Heating

11: SOCl₂ / 20 h / Ambient temperature

12: CH₂Cl₂ / 18 h / Ambient temperature

13: LiBH₄ / tetrahydrofuran / 19 h / 0 - 20 °C

14: H₂ / 10percent Pd/C / ethanol / 6 h / 760 Torr / Ambient temperature

15: acetic anhydride / tetrahydrofuran / 2 h / 60 - 70 °C

16: BH₃ / tetrahydrofuran / 3 h / 0 °C

17: 83 percent / 2,6-lutidine / 1,2-dichloro-ethane / 48 h / Heating

With 2,6-dimethylpyridine; chromium(VI) oxide; hydrogenchloride; triethylsilane; sodium tetrahydroborate; lithium borohydride; n-butyllithium; aluminium trichloride; thionyl chloride; Bromoform; sulfuric acid; borane; hydrogen; bromine; nitric acid; acetic anhydride; sodium hydride; acetic acid; triphenylphosphine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm970704s