2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

Base Information

Chemical Name:2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid
CAS No.:113976-28-6
Molecular Formula:C₂₃H₂₈N₈O₅
Molecular Weight:496.526
Hs Code.:

Synonyms:2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

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Chemical Property of 2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

Chemical Property:

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Technology Process of 2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

There total 8 articles about 2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56555-02-3
methyl 9-chloro-9-oxononanoate

: 113976-28-6
2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

Guidance literature:: Multi-step reaction with 6 steps

1: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

2: 3.5 h / Ambient temperature

3: NaN₃ / ethanol / 15 h / Heating

4: H₂, aq. HCl / Pd-C / ethanol / 17 h

5: Et₃N / dimethylformamide

6: 8 percent / aq. NaOH / methanol

With hydrogenchloride; sodium hydroxide; sodium azide; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In methanol; thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 2104-19-0
azelaic monomethyl ester

: 113976-28-6
2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

Guidance literature:: Multi-step reaction with 7 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

3: 3.5 h / Ambient temperature

4: NaN₃ / ethanol / 15 h / Heating

5: H₂, aq. HCl / Pd-C / ethanol / 17 h

6: Et₃N / dimethylformamide

7: 8 percent / aq. NaOH / methanol

With hydrogenchloride; sodium hydroxide; thionyl chloride; sodium azide; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In methanol; thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 6415-48-1
2-bromoazelaic acid dimethyl ester

: 113976-28-6
2-{4-[(2,4-Diamino-pteridin-6-ylmethyl)-amino]-benzoylamino}-nonanedioic acid

Guidance literature:: Multi-step reaction with 4 steps

1: NaN₃ / ethanol / 15 h / Heating

2: H₂, aq. HCl / Pd-C / ethanol / 17 h

3: Et₃N / dimethylformamide

4: 8 percent / aq. NaOH / methanol

With hydrogenchloride; sodium hydroxide; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014