C₂₅H₃₄O₂Si

Base Information

Chemical Name:C₂₅H₃₄O₂Si
CAS No.:1384271-72-0
Molecular Formula:C₂₅H₃₄O₂Si
Molecular Weight:394.629
Hs Code.:

C<sub>25</sub>H<sub>34</sub>O<sub>2</sub>Si

Synonyms:C₂₅H₃₄O₂Si

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Chemical Property of C₂₅H₃₄O₂Si

Chemical Property:

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Technology Process of C₂₅H₃₄O₂Si

There total 6 articles about C₂₅H₃₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₂O₃Si

: 2065-66-9
methyl-triphenylphosphonium iodide

: 1384271-72-0
C₂₅H₃₄O₂Si

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-75-3
C₂₉H₄₀O₃Si

: 1384271-72-0
C₂₅H₃₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

2.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

4.2: -78 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

With titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; ethanol; dichloromethane; ethylene glycol; 3.1: Sharpless epoxidation / 4.1: Swern oxidation / 4.2: Swern oxidation;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-73-1
C₁₃H₂₂O₃

: 1384271-72-0
C₂₅H₃₄O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

3.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

5.2: -78 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

With 1H-imidazole; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; In tetrahydrofuran; ethanol; dichloromethane; ethylene glycol; 4.1: Sharpless epoxidation / 5.1: Swern oxidation / 5.2: Swern oxidation;
DOI:10.1016/j.tetlet.2012.04.118