C₃₄H₅₂O₇⁽¹⁸⁾OSi

Base Information

Chemical Name:C₃₄H₅₂O₇⁽¹⁸⁾OSi
CAS No.:1264175-90-7
Molecular Formula:C₃₄H₅₂O₈Si
Molecular Weight:618.868
Hs Code.:

C<sub>34</sub>H<sub>52</sub>O<sub>7</sub><sup>(18)</sup>OSi

Synonyms:C₃₄H₅₂O₇⁽¹⁸⁾OSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₅₂O₇⁽¹⁸⁾OSi

Chemical Property:

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Technology Process of C₃₄H₅₂O₇⁽¹⁸⁾OSi

There total 17 articles about C₃₄H₅₂O₇⁽¹⁸⁾OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1264175-89-4
C₃₄H₅₂O₆⁽¹⁸⁾OSi

: 1264175-90-7
C₃₄H₅₂O₇⁽¹⁸⁾OSi

Guidance literature:: With bis(acetylacetonate)oxovanadium; Cumene hydroperoxide; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;
DOI:10.1021/ol103003f

Reference yield:

: 1264175-79-2
(2R,3S,E)-N,2,8-trimethoxy-N,4-dimethyl-3-((triethylsilyl)oxy)oct-4-enamide

: 1264175-90-7
C₃₄H₅₂O₇⁽¹⁸⁾OSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: diethyl ether / 0 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: calcium hydride / dichloromethane / 0.5 h / 23 °C

3.2: 0.33 h / -78 °C / Inert atmosphere

4.1: trifluoroacetic acid / tetrahydrofuran; water / 0.75 h / 23 °C / pH 2

5.1: hydrogenchloride; ¹⁸O-labeled water / tetrahydrofuran; diethyl ether / 2 h / 23 °C

6.1: bis(acetylacetonate)oxovanadium; Cumene hydroperoxide / dichloromethane / -78 - 0 °C / Inert atmosphere

With hydrogenchloride; calcium hydride; bis(acetylacetonate)oxovanadium; Cumene hydroperoxide; ¹⁸O-labeled water; triethylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ol103003f

Reference yield:

: (5R,6S)-8,8-diethyl-4-ethylidene-5-methoxy-6-((E)-6-methoxyhex-2-en-2-yl)-2,2-dimethyl-3,7-dioxa-2,8-disiladecane

: 1264175-90-7
C₃₄H₅₂O₇⁽¹⁸⁾OSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: calcium hydride / dichloromethane / 0.5 h / 23 °C

1.2: 0.33 h / -78 °C / Inert atmosphere

2.1: trifluoroacetic acid / tetrahydrofuran; water / 0.75 h / 23 °C / pH 2

3.1: hydrogenchloride; ¹⁸O-labeled water / tetrahydrofuran; diethyl ether / 2 h / 23 °C

4.1: bis(acetylacetonate)oxovanadium; Cumene hydroperoxide / dichloromethane / -78 - 0 °C / Inert atmosphere

With hydrogenchloride; calcium hydride; bis(acetylacetonate)oxovanadium; Cumene hydroperoxide; ¹⁸O-labeled water; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/ol103003f