decacarbonyl-μ-tetrachlorodiphosphinedichromium

Base Information

Chemical Name:decacarbonyl-μ-tetrachlorodiphosphinedichromium
CAS No.:90857-01-5
Molecular Formula:C₁₀Cl₄Cr₂O₁₀P₂
Molecular Weight:587.856
Hs Code.:

Synonyms:decacarbonyl-μ-tetrachlorodiphosphinedichromium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of decacarbonyl-μ-tetrachlorodiphosphinedichromium

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Technology Process of decacarbonyl-μ-tetrachlorodiphosphinedichromium

There total 1 articles about decacarbonyl-μ-tetrachlorodiphosphinedichromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: disodium decacarbonyldichromate

: 18461-41-1
((chloro)3phosphane)pentacarbonylchromium

: [(Cr(CO)5)2PCl]

: 90857-01-5
decacarbonyl-μ-tetrachlorodiphosphinedichromium

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; addn. of Na2(Cr2(CO)10) to (Cr(CO)5PCl3) in THF at -78°C, stirring for 1 h and slow warming to room temp.; evapn. (vac.), dissolving in benzene, filtn. (NaCl), evapn., dissolving in CH2Cl2, treating with silica gel, drying (vac.), column chromy. on silica gel, elution with n-hexane-toluene and extn. of the residue with n-pentane;