3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Base Information

Chemical Name:3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid
CAS No.:160982-42-3
Molecular Formula:C₂₃H₃₆I₃N₅O₄
Molecular Weight:827.283
Hs Code.:

Synonyms:3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

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Chemical Property of 3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

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Technology Process of 3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

There total 4 articles about 3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 111-40-0,98824-35-2
3-azapentane-1,5-diamine

: 160982-41-2
3-<<6-<(chloroacetyl)amino>-1-oxohexyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

: 160982-42-3
3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Guidance literature:: at 50 ℃; for 6h;

Reference yield: 48.0%

: 160982-42-3
3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Guidance literature:

Reference yield:

: 61435-75-4
6-<(chloroacetyl)amino>hexanoic acid

: 160982-42-3
3-<<6-<<<2-<(2-aminoethyl)amino>ethyl>amino>acetylamino>-1-oxoethyl>amino>-α-ethyl-2,4,6-triiodobenzenepropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl dichloride, 2.) pyridine / 1.) DMF, CH₂Cl₂, 5 deg C, 1 h, 2.) THF, CH₃CN, 5 deg C, then 40 deg C, 2 h, 3.) THF, reflux, 3 h

2: 48 percent / 6 h / 50 °C

With pyridine; oxalyl dichloride;