spiro

Base Information

Chemical Name:spiro
CAS No.:115984-02-6
Molecular Formula:C₂₂H₂₅NO₆S
Molecular Weight:431.51
Hs Code.:

spiro<methyl 4,6-O-benzylidene-2,3-dideoxy-β-D-arabino-hexopyranoside-2,2'-N-(p-tolylsulfonyl)aziridine>

Synonyms:spiro

Suppliers and Price of spiro

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of spiro

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of spiro

There total 8 articles about spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 115984-00-4,115984-01-5
methyl 2-C-(aminomethyl)-4,6-O-benzylidene-2,3-dideoxy-2-<(p-tolylsulfonyl)amino>-α-D-ribo-hexopyranoside

: 115984-02-6
spiro

Guidance literature:: With sodium nitrite; In acetic acid; for 1h;
DOI:10.1021/jo00254a048

Reference yield: 84.0%

: 115984-00-4,115984-01-5
methyl 2-C-(aminomethyl)-4,6-O-benzylidene-2,3-dideoxy-2-<(p-tolylsulfonyl)amino>-β-D-arabino-hexopyranoside

: 115984-02-6
spiro

Guidance literature:: With sodium nitrite; In acetic acid; for 1h;
DOI:10.1021/jo00254a048

Reference yield:

: 19272-50-5
Methyl-4,6-O-benzyliden-3-deoxy-α-D-erythro-hexo-pyranosid-2-ulose

: 115984-02-6
spiro

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / NH₃ / methanol / 72 h / 50 °C

2: 66 percent / pyridine / Ambient temperature

3: 58 percent / lithium aluminum hydride / dioxane / 1 h / Ambient temperature

4: 89 percent / sodium nitrite / aq. acetic acid / 1 h

With pyridine; lithium aluminium tetrahydride; ammonia; sodium nitrite; In 1,4-dioxane; methanol; acetic acid;
DOI:10.1021/jo00254a048