Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

Base Information

Chemical Name:Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester
CAS No.:223771-35-5
Molecular Formula:C₁₄H₂₇NO₅S
Molecular Weight:321.438
Hs Code.:

Synonyms:Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

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Chemical Property of Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

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Technology Process of Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

There total 5 articles about Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1877-72-1
3-Cyanobenzoic acid

: 223771-35-5
Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: NH₃ / Raney Ni / ethanol / 51714.8 Torr

2: aq. NaOH / dioxane

3: H₂, AcOH / PtO₂ / 2585.7 Torr

5: BH₃ / tetrahydrofuran

6: DMAP, i-Pr₂NEt / CH₂Cl₂

With dmap; sodium hydroxide; borane; ammonia; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; nickel; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane;
DOI:10.1021/jm980194h

Reference yield:

: 2393-20-6
3-aminomethylbenzoic acid

: 223771-35-5
Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: aq. NaOH / dioxane

2: H₂, AcOH / PtO₂ / 2585.7 Torr

4: BH₃ / tetrahydrofuran

5: DMAP, i-Pr₂NEt / CH₂Cl₂

With dmap; sodium hydroxide; borane; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1021/jm980194h

Reference yield:

: 117445-22-4
3-(tert-butoxycarbonylamino-methyl)benzoic acid

: 223771-35-5
Methanesulfonic acid (1R,3S)-3-(tert-butoxycarbonylamino-methyl)-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, AcOH / PtO₂ / 2585.7 Torr

3: BH₃ / tetrahydrofuran

4: DMAP, i-Pr₂NEt / CH₂Cl₂

With dmap; borane; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm980194h