ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

Base Information

Chemical Name:ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate
CAS No.:1632161-92-2
Molecular Formula:C₃₁H₃₇NO₈
Molecular Weight:551.637
Hs Code.:

Synonyms:ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

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Technology Process of ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

There total 2 articles about ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1632161-91-1
ethyl 4-[[6-(aminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

: 501-53-1,94274-21-2
benzyl chloroformate

: 1632161-92-2
ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c4md00032c

Reference yield:

: 1632161-90-0
ethyl 4-[[6-cyano-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

: 1632161-92-2
ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; ammonia / N,N-dimethyl-formamide; ethanol / 48 h / 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C

With ammonia; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c4md00032c

Reference yield: 96.0%

: 1632161-92-2
ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate

: 1632161-93-3
4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-hydroxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoic acid

Guidance literature:: ethyl 4-[[6-(benzyloxycarbonylaminomethyl)-7-(4-ethoxy-4-oxo-butoxy)-2-naphthyl]oxy]butanoate; With sodium hydroxide; In methanol; at 20 ℃; for 3.5h;

With hydrogenchloride; In water;
DOI:10.1039/c4md00032c