C₂₃H₃₀O₆S

Base Information

Chemical Name:C₂₃H₃₀O₆S
CAS No.:1548667-87-3
Molecular Formula:C₂₃H₃₀O₆S
Molecular Weight:434.554
Hs Code.:

C<sub>23</sub>H<sub>30</sub>O<sub>6</sub>S

Synonyms:C₂₃H₃₀O₆S

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Chemical Property of C₂₃H₃₀O₆S

Chemical Property:

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Technology Process of C₂₃H₃₀O₆S

There total 5 articles about C₂₃H₃₀O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1548667-83-9
C₁₆H₂₄O₄

: 98-59-9
p-toluenesulfonyl chloride

: 1548667-87-3
C₂₃H₃₀O₆S

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo4025545

Reference yield:

: 183722-51-2
((2R,3S)-3-(4-methoxybenzyloxy)tetrahydro-2H-pyran-2-yl)methanol

: 1548667-87-3
C₂₃H₃₀O₆S

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 0.33 h / 0 °C

2: toluene / 43 h / 20 °C

3: nickel dichloride; sodium tetrahydroborate / methanol / 0 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

5: triethylamine; dmap / dichloromethane / 3 h / 20 °C

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfur trioxide pyridine complex; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo4025545

Reference yield:

: 410531-68-9
(2S,3S)-3-(4-Methoxy-benzyloxy)-tetrahydro-pyran-2-carbaldehyde

: 1548667-87-3
C₂₃H₃₀O₆S

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 43 h / 20 °C

2: nickel dichloride; sodium tetrahydroborate / methanol / 0 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4: triethylamine; dmap / dichloromethane / 3 h / 20 °C

With dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine; nickel dichloride; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo4025545