1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

Base Information

Chemical Name:1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)
CAS No.:155928-95-3
Molecular Formula:C₄₆H₇₄N₈O₆S₃
Molecular Weight:931.342
Hs Code.:

Synonyms:1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

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Chemical Property of 1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

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Technology Process of 1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

There total 4 articles about 1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 155928-94-2
2-(4,8,11-trimethyl-1,4,8,11-tetraazacyclotetradec-1-yl)-1-(4,8,11-tritosyl-1,4,8,11-tetraazacyclotetradec-1-yl)ethan-1-one

: 155928-95-3
1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

Guidance literature:: With borane; In tetrahydrofuran; dichloromethane; for 24h; Heating;
DOI:10.1002/hlca.19940770105

Reference yield:

: 67707-85-1
1,4,8-trimethyl-1,4,8,11-tetraazacyclotetradecane

: 155928-95-3
1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / Na₂CO₃ / acetonitrile / 24 h / Heating

2: 68 percent / 1 M BH₃ / CH₂Cl₂; tetrahydrofuran / 24 h / Heating

With borane; sodium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/hlca.19940770105

Reference yield:

: 104395-69-9
tris-(p-toluenesulfonyl)-1,4,8,11-tetraazacyclotetradecane

: 155928-95-3
1,1'-(ethane-1,2-diyl)-4,8,11-trimethyl-4',8',11'-tritosylbis(1,4,8,11-tetraazacyclotetradecane)

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / Et₃N / CH₂Cl₂ / 0.5 h / -7 °C

2: 64 percent / Na₂CO₃ / acetonitrile / 24 h / Heating

3: 68 percent / 1 M BH₃ / CH₂Cl₂; tetrahydrofuran / 24 h / Heating

With borane; sodium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/hlca.19940770105