(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

Base Information

Chemical Name:(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate
CAS No.:1300748-82-6
Molecular Formula:C₃₄H₂₈N₂O₂
Molecular Weight:496.609
Hs Code.:

Synonyms:(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

Suppliers and Price of (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

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Technology Process of (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

There total 4 articles about (E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 102-92-1,17082-09-6
cinnamoyl chloride

: 199007-50-6
1-(1-Trityl-1H-imidazol4-yl)propen-3-ol

: 1300748-82-6
(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

Guidance literature:: 1-(1-Trityl-1H-imidazol4-yl)propen-3-ol; With sodium hydride; In tetrahydrofuran; mineral oil; for 1h; Inert atmosphere; Cooling with ice;

cinnamoyl chloride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere; Cooling with ice;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: 112606-55-0
C₂₆H₂₂N₂O₂

: 1300748-82-6
(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisobutylaluminium hydride

2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

2.2: 20 °C / Inert atmosphere; Cooling with ice

2.3: 20 °C / Inert atmosphere

With sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300748-82-6
(E)-3-(1-triphenylmethylimidazol-4-yl)-2-propenyl (E)-3-phenyl-2-propenoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid; magnesium sulfate / Reflux

2.1: triethylamine / N,N-dimethyl-formamide

3.1: diisobutylaluminium hydride

4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / Inert atmosphere; Cooling with ice

4.2: 20 °C / Inert atmosphere; Cooling with ice

4.3: 20 °C / Inert atmosphere

With sulfuric acid; sodium hydride; diisobutylaluminium hydride; magnesium sulfate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; 1.1: Fischer esterification;
DOI:10.1039/c0ob00657b