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Technology Process of (CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

Base Information Edit
  • Chemical Name:(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO
  • CAS No.:899421-92-2
  • Molecular Formula:C40H66N2O5Si
  • Molecular Weight:683.06
  • Hs Code.:
  • Mol file:899421-92-2.mol
(CH<sub>2</sub>)10CCH<sub>2</sub>OCH(CH<sub>2</sub>)3O((C(CH<sub>3</sub>)3)(CH<sub>3</sub>)2Si)(CH<sub>2</sub>CHCH<sub>2</sub>NCCHCH)CH<sub>2</sub>CH<sub>2</sub>NCH(OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CHO

Synonyms:(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

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Chemical Property of (CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO Edit
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Technology Process of (CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

There total 3 articles about (CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

C<sub>40</sub>H<sub>68</sub>N<sub>2</sub>O<sub>5</sub>Si
899421-91-1

C40H68N2O5Si

(CH<sub>2</sub>)10CCH<sub>2</sub>OCH(CH<sub>2</sub>)3O((C(CH<sub>3</sub>)3)(CH<sub>3</sub>)2Si)(CH<sub>2</sub>CHCH<sub>2</sub>NCCHCH)CH<sub>2</sub>CH<sub>2</sub>NCH(OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CHO
899421-92-2

(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

Guidance literature:
With 2-iodoxybenzoic aid; In dimethyl sulfoxide; at 23 ℃; for 1.75h;
DOI:10.1021/ja074300t

Reference yield:

C<sub>30</sub>H<sub>48</sub>N<sub>2</sub>O<sub>4</sub>
848731-55-5

C30H48N2O4

(CH<sub>2</sub>)10CCH<sub>2</sub>OCH(CH<sub>2</sub>)3O((C(CH<sub>3</sub>)3)(CH<sub>3</sub>)2Si)(CH<sub>2</sub>CHCH<sub>2</sub>NCCHCH)CH<sub>2</sub>CH<sub>2</sub>NCH(OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CHO
899421-92-2

(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

Guidance literature:
Multi-step reaction with 2 steps
1: benzene / Heating
2: iodoxybenzoic acid / dimethylsulfoxide
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; benzene;
DOI:10.1002/anie.200600417

Reference yield:

4-(tert-butyldimethylsilanyloxy)butanal
87184-81-4

4-(tert-butyldimethylsilanyloxy)butanal

(CH<sub>2</sub>)10CCH<sub>2</sub>OCH(CH<sub>2</sub>)3O((C(CH<sub>3</sub>)3)(CH<sub>3</sub>)2Si)(CH<sub>2</sub>CHCH<sub>2</sub>NCCHCH)CH<sub>2</sub>CH<sub>2</sub>NCH(OCH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>)CHO
899421-92-2

(CH2)10CCH2OCH(CH2)3O((C(CH3)3)(CH3)2Si)(CH2CHCH2NCCHCH)CH2CH2NCH(OCH2C6H4OCH3)CHO

Guidance literature:
Multi-step reaction with 2 steps
1: benzene / Heating
2: iodoxybenzoic acid / dimethylsulfoxide
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; benzene;
DOI:10.1002/anie.200600417
upstream raw materials:

C40H68N2O5Si

C30H48N2O4

4-(tert-butyldimethylsilanyloxy)butanal

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