ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Base Information

Chemical Name:ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate
CAS No.:1544740-98-8
Molecular Formula:C₃₄H₃₈N₂O₄
Molecular Weight:538.687
Hs Code.:

ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Synonyms:ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

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Chemical Property of ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

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Technology Process of ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

There total 4 articles about ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1544740-97-7
5-(4-bromo-3,5-dimethylphenoxy)-2,2-dimethylpentanenitrile

: 1544739-26-5
(5aR,6S,6aS)-ethyl 3-((3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl)oxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

: 1544740-98-8
ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; In tetrahydrofuran; water; at 100 ℃; for 18h; Inert atmosphere;

Reference yield:

: 108-68-9,50356-23-5
3,5-Dimethylphenol

: 1544740-98-8
ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 18 h / Reflux

2: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

3: N-Bromosuccinimide / dichloromethane / 18 h / 15 °C

4: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 18 h / 100 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; sodium carbonate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; water; acetone;

Reference yield:

: 3245-53-2
3-bromo-1-(3,5-dimethylphenoxy)propane

: 1544740-98-8
ethyl 3-((4’-((4-cyano-4-methylpentyl)oxy)-2’,6’-dimethyl-[1,1’-biphenyl]-3-yl)methoxy)-5,5a,6,6a-tetrahydrocyclopropa[4,5]cyclopenta[1,2-c]pyridine-6-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium diisopropyl amide / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2: N-Bromosuccinimide / dichloromethane / 18 h / 15 °C

3: sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran; water / 18 h / 100 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; sodium carbonate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; water;