N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine

Base Information

• Chemical Name: N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine
• CAS No.: 1246254-60-3
• Molecular Formula: C₃₈H₄₇N₃O₇Si
• Molecular Weight: 685.893

Synonyms:N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine

Chemical Property of N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine

Chemical Property:

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Technology Process of N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine

There total 1 articles about N₄-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

C45H51N3O9SSi (1246254-59-0) → N4-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine (1246254-60-3)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 20 - 120 ℃; Inert atmosphere; Reflux;

Reference yield: 58.2%

N4-acetyl-2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine (1246254-60-3) → 2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine (1246254-61-4)

Guidance literature:

With ammonia; In methanol; at 20 ℃;

upstream raw materials:

C₄₅H₅₁N₃O₉SSi

Downstream raw materials:

2'-O-(t-butyldimethylsilyl)-3'-deoxy-5'-O-(4,4'-dimethoxytrityl)cytidine

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