(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

Base Information

Chemical Name:(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide
CAS No.:1150658-29-9
Molecular Formula:C₂₉H₃₄N₂O₄
Molecular Weight:474.6
Hs Code.:

Synonyms:(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

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Chemical Property of (E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

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Technology Process of (E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

There total 2 articles about (E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1150658-28-8
(E)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enoic acid

: 4-(2-(dimethylamino)ethoxy)aniline dihydrochloride

: 1150658-29-9
(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

Guidance literature:: (E)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enoic acid; 4-(2-(dimethylamino)ethoxy)aniline dihydrochloride; With dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In dichloromethane; at 0 ℃; for 0.166667h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 15.0833h; Product distribution / selectivity;

Reference yield: 43.0%

: 1150658-28-8
(E)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enoic acid

: 1150658-29-9
(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 18h; Product distribution / selectivity;

Reference yield: 91.0%

: 1150658-29-9
(E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide

: 651329-50-9
(E)-2-(4-hydroxyphenyl)-3-phenylpent-2-enoic acid [4-(2-dimethylaminoethoxy)-phenyl] amide

Guidance literature:: (E)-N-(4-(2-(dimethylamino)ethoxy)phenyl)-2-(4-(methoxymethoxy)phenyl)-3-phenylpent-2-enamide; With hydrogenchloride; methanol; In ethyl acetate; at 20 ℃; for 2h;

With water; sodium hydrogencarbonate; In methanol; ethyl acetate; Product distribution / selectivity;