(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

Base Information

Chemical Name:(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate
CAS No.:897398-09-3
Molecular Formula:C₃₆H₄₂O₆
Molecular Weight:570.726
Hs Code.:

Synonyms:(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

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Chemical Property of (Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

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Technology Process of (Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

There total 5 articles about (Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 897398-20-8
(Z)-5-(hydroxymethyl)-3-[4-methyl-3-(methylethyl)pentylidene]-5-[(phenylmethoxy)methyl]-4,5-dihydrofuran-2-one

: 61535-46-4
3-benzyloxy-benzoyl chloride

: 897398-09-3
(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jm060011o

Reference yield:

: 897398-00-4
(Z)-5-[(4-methoxyphenoxy)methyl]-3-[4-methyl-3-(methylethyl)pentylidene]-5-[(phenylmethoxy)methyl]-4,5-dihydrofuran-2-one

: 897398-09-3
(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.5 h / 0 °C

2: 84 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; ammonium cerium(IV) nitrate; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1021/jm060011o

Reference yield:

: 897398-29-7
3-[1-hydroxy-4-methyl-3-(methylethyl)pentyl]-5-[(4-methoxyphenoxy)methyl]-5-[(phenylmethoxy)methyl]-3,4,5-trihydrofuran-2-one

: 897398-09-3
(Z)-{4-[4-methyl-3-(methylethyl)pentylidene]-5-oxo-2-[(phenylmethoxy)methyl]-2,3-dihydrofur-2-yl}methyl 3-(phenylmethoxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N; MsCl / CH₂Cl₂ / 0.5 h / 20 °C

1.2: 39 percent / diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 20 °C

2.1: 49 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.5 h / 0 °C

3.1: 84 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

With dmap; ammonium cerium(IV) nitrate; methanesulfonyl chloride; triethylamine; In dichloromethane; water; acetonitrile;
DOI:10.1021/jm060011o