trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

Base Information

Chemical Name:trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene
CAS No.:1426820-11-2
Molecular Formula:C₂₆H₃₀S₂
Molecular Weight:406.656
Hs Code.:

Synonyms:trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

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Chemical Property of trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

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Technology Process of trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

There total 8 articles about trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 57728-82-2
2-(methylthio)phenyl trifluoromethanesulfonate

: 1426819-93-3
6-(1-methylpentyl)-3-methylthio-2-naphthyl trifluoromethanesulfonate

: 14275-61-7,15979-38-1,118855-16-6
(E)-1,2-bis(tri-n-butylstannyl)ethene

: 1426820-11-2
trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 100 ℃; for 14h; Inert atmosphere; Darkness;

Reference yield:

: 1426819-90-0
2-methoxy-6-(1-methylpentyl)naphthalene

: 1426820-11-2
trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 1.25 h / -78 - 20 °C / Inert atmosphere

1.2: 15 h / -78 - 20 °C / Inert atmosphere

2.1: boron tribromide / dichloromethane / 19 h / -78 - 20 °C / Inert atmosphere

3.1: pyridine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 14 h / 100 °C / Inert atmosphere; Darkness

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; boron tribromide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1426819-91-1
2-methoxy-3-methylthio-(6-(1-methylpentyl)naphthalene)

: 1426820-11-2
trans-1-(6-(1-methylpentyl)-3-(methylthio)naphthalen-2-yl)-2-(2-(methylthio)phenyl)ethene

Guidance literature:: Multi-step reaction with 3 steps

1: boron tribromide / dichloromethane / 19 h / -78 - 20 °C / Inert atmosphere

2: pyridine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 14 h / 100 °C / Inert atmosphere; Darkness

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; In dichloromethane; N,N-dimethyl-formamide;