3-Methyl-2-p-tolylimino-benzothiazoline

Base Information

Chemical Name:3-Methyl-2-p-tolylimino-benzothiazoline
CAS No.:70038-60-7
Molecular Formula:C15H14N2S
Molecular Weight:254.356
Hs Code.:
DSSTox Substance ID:DTXSID10356949
Mol file:70038-60-7.mol

Synonyms:3-Methyl-2-p-tolylimino-benzothiazoline;70038-60-7;3-methyl-N-(4-methylphenyl)-1,3-benzothiazol-2-imine;DTXSID10356949;3-methyl-2-p-tolyliminobenzothiazoline;FT-0765535;AN-689/41741260;4-methyl-N-(3-methyl-1,3-benzothiazol-2(3H)-ylidene)aniline;(2Z)-3-Methyl-N-(4-methylphenyl)-1,3-benzothiazol-2(3H)-imine;(E)-4-methyl-N-(3-methylbenzo[d]thiazol-2(3H)-ylidene)aniline;BENZENAMINE,4-METHYL-N-(3-METHYL-2(3H)-BENZOTHIAZOLYLIDENE)-

Suppliers and Price of 3-Methyl-2-p-tolylimino-benzothiazoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-METHYL-2-P-TOLYLIMINO-BENZOTHIAZOLINE 95.00%
5MG
$ 499.00

Total 7 raw suppliers

Chemical Property of 3-Methyl-2-p-tolylimino-benzothiazoline

Chemical Property:

Vapor Pressure:4.79E-07mmHg at 25°C
Melting Point:126 °C(Solv: ethanol (64-17-5))
Refractive Index:1.643
Boiling Point:413.5 °C at 760 mmHg
PKA:4.76±0.20(Predicted)
Flash Point:203.9 °C
PSA：45.53000
Density:1.17 g/cm³
LogP:3.78060
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:254.08776963
Heavy Atom Count:18
Complexity:321

Purity/Quality:

98%Min ^*data from raw suppliers

3-METHYL-2-P-TOLYLIMINO-BENZOTHIAZOLINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=C2N(C3=CC=CC=C3S2)C

Technology Process of 3-Methyl-2-p-tolylimino-benzothiazoline

There total 5 articles about 3-Methyl-2-p-tolylimino-benzothiazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 20064-98-6
2-methylthio-3-methylbenzothiazolium iodide

: 106-49-0,12221-03-3
p-toluidine

: 70038-60-7
3-methyl-2-(p-tolylimino)-2,3-dihydrobenzothiazole

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 8h;

Reference yield:

: 70038-58-3
3-methyl-3H-benzothiazol-2-one O-trimethylsilanyl-oxime

: 70038-60-7
3-methyl-2-(p-tolylimino)-2,3-dihydrobenzothiazole

Guidance literature:: Multi-step reaction with 3 steps

1: PhLi / diethyl ether; benzene

2: Et₃N

3: diethyl ether; benzene / Ambient temperature

With phenyllithium; triethylamine; In diethyl ether; benzene;
DOI:10.1246/bcsj.52.263

Reference yield:

: 30761-23-0
N-methylbenzothiazol-2-one-oxime

: 70038-60-7
3-methyl-2-(p-tolylimino)-2,3-dihydrobenzothiazole

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N

2: diethyl ether; benzene / Ambient temperature

With triethylamine; In diethyl ether; benzene;
DOI:10.1246/bcsj.52.263