Technology Process of C33H56O8Si
There total 24 articles about C33H56O8Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; acetic acid;
In
tetrahydrofuran;
at 20 ℃;
for 47h;
DOI:10.1021/ol400408w
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 25 h / 20 °C
2: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 47 h / 20 °C
With
palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; acetic acid;
In
tetrahydrofuran; methanol;
DOI:10.1021/ol400408w
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 0 - 20 °C
2: triethylamine / tetrahydrofuran / 0.83 h / 0 - 20 °C
3: dmap / toluene / 1.5 h / 20 °C
4: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 140 °C
5: palladium 10% on activated carbon; hydrogen / methanol / 25 h / 20 °C
6: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 47 h / 20 °C
With
dmap; Hoveyda-Grubbs catalyst second generation; lithium hydroxide monohydrate; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; acetic acid; triethylamine; p-benzoquinone;
In
tetrahydrofuran; methanol; water; toluene;
2: |Yamaguchi Lactonization;
DOI:10.1021/ol400408w
