[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄

Base Information

• Chemical Name: [Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄
• CAS No.: 84190-63-6
• Molecular Formula: C₅₈H₅₁O₂P₃Rh*ClO₄
• Molecular Weight: 1075.32

Synonyms:[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄

Chemical Property of [Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄

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Technology Process of [Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄

There total 3 articles about [Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(CO)(OP(CH₃C₆H₄)3)(P(C₆H₅)3)2]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Rh((CHCHC2H4)2)(OP(CH3C6H4)3)2](1+)*ClO4(1-)=[Rh((CHCHC2H4)2)(OP(CH3C6H4)3)2]ClO4 (84190-87-4) → [Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2]ClO4 (84190-63-6)

Guidance literature:

With CO; PPh₃; In dichloromethane; CO bubbled through complex soln. at room temp., PPh3 added, stirred for30 min; evapd., suspended in hexane, filtered off, washed with hexane, dried (vac.); elem. anal.;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

tri(4-methylphenyl)phosphine oxide (797-70-6) → [Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2]ClO4 (84190-63-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: CO; PPh₃ / dichloromethane

With CO; PPh₃; In dichloromethane; acetone;

DOI:10.1016/S0022-328X(00)85856-8

Reference yield:

[CO(P(C6H5)3)2RhCH3COCH3](1+)*ClO4(1-) = [CO(P(C6H5)3)2RhCH3COCH3]ClO4 (75214-93-6,32334-51-3) + tri(4-methylphenyl)phosphine oxide (797-70-6) → [Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2](1+)*ClO4(1-)=[Rh(CO)(OP(CH3C6H4)3)(P(C6H5)3)2]ClO4 (84190-63-6)

Guidance literature:

In acetone; stoich. amt. of ligand added to complex soln. at room temp.; concd., pptd. with hexane, filtered off, washed with hexane or ether, dried (vac.);

DOI:10.1016/S0022-328X(00)85856-8

upstream raw materials:

[CO(P(C₆H₅)3)2RhCH₃COCH₃]⁽¹⁺⁾*ClO₄^(1-) = [CO(P(C₆H₅)3)2RhCH₃COCH₃]ClO₄

tri(4-methylphenyl)phosphine oxide

[Rh((CHCHC₂H₄)2)(OP(CH₃C₆H₄)3)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh((CHCHC₂H₄)2)(OP(CH₃C₆H₄)3)2]ClO₄

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