19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

Base Information

Chemical Name:19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol
CAS No.:120577-96-0
Molecular Formula:C₃₂H₄₇NO₄
Molecular Weight:509.729
Hs Code.:

Synonyms:19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

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Chemical Property of 19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

Chemical Property:

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Technology Process of 19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

There total 4 articles about 19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 120577-97-1
19-(2-Bromo-5-dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

: 120577-96-0
19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

: 119056-03-0
C₃₂H₄₇NO₄

Guidance literature:: With tri-n-butyl-tin hydride; In toluene; at -78 ℃; for 0.333333h;

Reference yield:

: 119056-02-9
19-(2-chloro-5-dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

: 120577-96-0
19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

Guidance literature:: palladium; In methanol; hexane; dichloromethane; ammonium formate; ethyl acetate;

Reference yield:

: 120577-93-7
C₉H₁₁Cl₂MgN

: 120577-96-0
19-(3-Dimethylaminophenyl)-3,3-(2,2-dimethyltrimethylenedioxy)-9(11)-androstene-5α,17β-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent

2: Li / tetrahydrofuran; liquid ammonia / 0.33 h / -78 °C

With lithium; In tetrahydrofuran; ammonia;