(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

Base Information

Chemical Name:(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol
CAS No.:1054682-27-7
Molecular Formula:C₅₉H₇₆FN₃O₇
Molecular Weight:958.267
Hs Code.:

Synonyms:(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

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Technology Process of (2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

There total 6 articles about (2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 866030-92-4
3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl fluoride

: 202812-10-0
(2S,3S,4S)-2-azido-3,4-di-O-benzyl-octadecan-1,3,4-triol

: (2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-β-D-galactopyranosyl)-1,3,4-octadecanetriol

: 1054682-27-7
(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

Guidance literature:: With silver perchlorate; tin(IV) chloride; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/ejoc.200500053

Reference yield: 16.0%

: 866030-91-3
3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-β-D-galactopyranosyl acetate

: 160280-67-1
(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-trityl-1,3,4-octadecanetriol

: (2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-β-D-galactopyranosyl)-1,3,4-octadecanetriol

: 1054682-27-7
(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

Guidance literature:: With silver perchlorate; tin(IV) chloride; In diethyl ether; at 20 ℃; for 14h;
DOI:10.1002/ejoc.200500053

Reference yield:

: 2-deoxy-2-fluoro-3,4,6-tri-O-benzyl-α,β-D-galactopyranose

: 1054682-27-7
(2S,3S,4R)-2-azido-3,4-di-O-benzyl-1-O-(3,4,6-tri-O-benzyl-2-deoxy-2-fluoro-α-D-galactopyranosyl)-1,3,4-octadecanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: DAST / tetrahydrofuran / 0.5 h / 20 °C

2: 28 percent / SnCl₄; AgClO₄ / tetrahydrofuran / 12 h / 20 °C

With silver perchlorate; tin(IV) chloride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In tetrahydrofuran; 2: Mukaiyama reaction;
DOI:10.1002/ejoc.200500053