C₃₀H₄₀N₂

Base Information

Chemical Name:C₃₀H₄₀N₂
CAS No.:1410790-06-5
Molecular Formula:C₃₀H₄₀N₂
Molecular Weight:428.661
Hs Code.:

C<sub>30</sub>H<sub>40</sub>N<sub>2</sub>

Synonyms:C₃₀H₄₀N₂

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Chemical Property of C₃₀H₄₀N₂

Chemical Property:

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Technology Process of C₃₀H₄₀N₂

There total 15 articles about C₃₀H₄₀N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1410789-68-2
1-methyl-4{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylacetyl}pirerazine

: 1410790-06-5
C₃₀H₄₀N₂

Guidance literature:: 1-methyl-4{4-[α-(1-tricyclo[3.3.1.1^3,7]decyl)phenylmethyl]phenylacetyl}pirerazine; With lithium aluminium tetrahydride; In tetrahydrofuran; for 3h; Reflux;

With sodium hydroxide; In tetrahydrofuran; ethanol; water; at 0 ℃;
DOI:10.1021/jm3013008

Reference yield: 63.0%

: 1410789-59-1
α-{4-[2-(4-methyl-1-piperazinyl)ethyl]phenyl}-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol

: 1410790-06-5
C₃₀H₄₀N₂

Guidance literature:: α-{4-[2-(4-methyl-1-piperazinyl)ethyl]phenyl}-α-phenyl-1-tricyclo[3.3.1.1^3,7]decanemethanol; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.25h; Inert atmosphere;

With triethylsilane; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With sodium carbonate; In dichloromethane; water; at 0 ℃; Inert atmosphere;
DOI:10.1021/jm3013008

Reference yield:

: 31919-47-8
1-benzoyladamantane

: 1410790-06-5
C₃₀H₄₀N₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: magnesium / diethyl ether / Inert atmosphere; Reflux

1.2: 0 °C / Inert atmosphere

2.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C / Inert atmosphere

2.3: 0 °C

3.1: n-butyllithium / tetrahydrofuran; hexane; N,N-dimethyl-formamide / 2 h / -80 - 20 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux

4.2: 0 °C

5.1: thionyl chloride; calcium carbonate; calcium chloride / diethyl ether / 12 h / 20 °C

6.1: dimethyl sulfoxide / 12 h / 20 °C / Inert atmosphere

7.1: hydrogenchloride; water / 3 h / Reflux

8.1: sodium hydroxide / ethanol; water / 2 h / Reflux

8.2: 0 °C

9.1: thionyl chloride / 1 h / 60 °C

10.1: tetrahydrofuran / 12 h / 0 - 20 °C / Reflux

11.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux

11.2: 0 °C

With hydrogenchloride; lithium aluminium tetrahydride; n-butyllithium; thionyl chloride; water; magnesium; trifluoroacetic acid; calcium carbonate; calcium chloride; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm3013008