2-benzylidene-1-tetralinthione dimer

Base Information

• Chemical Name: 2-benzylidene-1-tetralinthione dimer
• CAS No.: 67254-58-4
• Molecular Formula: C₃₄H₂₈S₂
• Molecular Weight: 500.728

Synonyms:2-benzylidene-1-tetralinthione dimer

Chemical Property of 2-benzylidene-1-tetralinthione dimer

Chemical Property:

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Technology Process of 2-benzylidene-1-tetralinthione dimer

There total 2 articles about 2-benzylidene-1-tetralinthione dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2-benzylidene-1-tetralone (6261-32-1) → 2-benzylidene-1-tetralinthione dimer (67254-58-4)

Guidance literature:

With Lawessons reagent; In benzene; Heating;

DOI:10.1246/cl.1982.793

Reference yield:

→ 2-benzylidene-1-tetralinthione dimer (67254-58-4)

Guidance literature:

Benzyliden-1-tetralon, P4S10;

DOI:10.1021/jo00415a036

Reference yield: 83.0%

2-benzylidene-1-tetralinthione dimer (67254-58-4) + tetraphenylallene (1674-18-6) → 3,3,4-Triphenyl-2-(diphenylmethylene)-5,6-dihydrobenzothiochroman (72478-89-8)

Guidance literature:

In benzene; for 0.583333h; Heating;

DOI:10.1021/jo01294a001

upstream raw materials:

(E)-2-benzylidene-1-tetralone

Downstream raw materials:

1,3-Diphenyl-2-((E)-styryl)-2,3,9,10-tetrahydro-1H-4-thia-phenanthrene

3,3,4-Triphenyl-2-(diphenylmethylene)-5,6-dihydrobenzothiochroman

3,3,4-Triphenyl-5,6-dihydrobenzothiochroman-2-one

2-Isopropenyl-1-phenyl-2,3,9,10-tetrahydro-1H-4-thia-phenanthrene 4-oxide

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